SBIR-STTR Award

MEMS Resonant Nanobalance Dew Point Meters
Award last edited on: 11/20/2017

Sponsored Program
SBIR
Awarding Agency
NSF
Total Award Amount
$900,000
Award Phase
2
Solicitation Topic Code
EI
Principal Investigator
Paul Neilson

Company Information

FemtoScale Inc (AKA: Femto Scale Inc)

3888 E Mexico Avenue Suite 254
Denver, CO 80210
   (303) 881-7359
   info@femtoscale.com
   www.femtoscale.com
Location: Single
Congr. District: 01
County: Denver

Phase I

Contract Number: ----------
Start Date: ----    Completed: ----
Phase I year
2012
Phase I Amount
$150,000
This Small Business Innovation Research (SBIR) Phase I project aims to develop a micro-electro-mechanical-systems (MEMS) based moisture (dew point) measurement instrument. Measurements of trace moisture are needed in a variety of different industrial sectors, including semiconductor manufacturing, pure gas supply, atmospheric and climate research, aerospace, petrochemical processing, power generation, air filter and purifier manufacturing, and supply of reference standards for other trace gases. Most of the commercially available moisture sensors lack the required accuracy, sensitivity, and responsiveness for many existing applications, or are too costly. The proposed approach utilizes micro-electro-mechanical resonant balances coupled with a cooling element. The instrument will measure dew point using the standard chilled surface technique to deposit a layer of moisture on the surface of the resonant balances. Mass of the deposited moisture causes a shift in the resonant frequency of the micro-resonator that indicates reaching the dew point. Because the nanobalances are capable of weighing as little as a few femto-grams of deposited moisture, only a very small amount of gas needs to be chilled to deposit sufficient water to indicate the dew point. Preliminary prototype assembly and reliability and response time characterizations will be performed in this Phase I effort. The broader impact/commercial potential of this project is development of more accurate, responsive, stable, robust, and versatile moisture measurement instruments than currently available instruments at the same price range. Chilled mirror dew point sensors generally provide higher accuracy compared to other categories of moisture sensors. Such devices however suffer from long response times and vulnerability of their optical sensing mechanism to debris and contamination. The proposed MEMS based technology combines the advantages of the chilled mirror sensors along with faster response and improved robustness provided by the MEMS resonant nanobalances. The reduced chilling needs allow for faster response to changes in moisture content, reduced power consumption for the cooler and novel uses such as battery powered spot sampling systems. An important immediate market for the proposed instrument with great national significance is the measurement of moisture in natural gas. In cold climates excess water in the gas pipeline can freeze the pipe shut, rendering the pipeline useless until the frozen point can be located and cleared. The battery powered, spot checking, robust operation and low cost nature of the proposed instrument will allow widespread use in the upstream Natural Gas pipeline system to measure moisture at points of custody transfer.

Phase II

Contract Number: ----------
Start Date: ----    Completed: ----
Phase II year
2013
Phase II Amount
$750,000
This Small Business Innovation Research (SBIR) Phase II project aims to develop a micro-electro-mechanical system (MEMS)-based moisture (dew point) measurement instrument. Trace moisture measurements are needed in a variety of industrial sectors including natural gas production and distribution, semiconductor manufacturing, pure gas supply, aerospace, and petrochemical processing. Commercially-available moisture sensors are either very expensive, or alternatively lack the required accuracy, long-term stability, and responsiveness for many existing applications. The innovative aspect of the proposed approach is the utilization of micro-electro-mechanical resonant balances coupled with a cooling element. The instrument will measure dew point using the highly accurate chilled surface technique to deposit a layer of moisture on the surface of the resonant balances, hence combining the accuracy of the chilled surface measurement technique the with small size, low power consumption and affordability enabled by MEMS. The MEMS resonant balances are capable of detecting as little as a few femto-grams of deposited moisture. Therefore, only a very small amount of gas needs to be chilled for a short period of time (i.e. low power/battery operation) to deposit sufficient water to indicate the dew point. The self-zeroing capability of the measurement technique eliminates the need for frequent maintenance and calibration.

The broader impact/commercial potential of this project includes a significant leap forward in the moisture measurement technologies that have experienced no major development over the past several decades. The proposed new class of dew pointers offers higher accuracy, responsiveness, stability, and robustness currently unavailable at the same price range. An important immediate market with great national significance is the measurement of moisture in natural gas. In cold climates excess water in the gas pipeline can freeze the pipe shut, rendering the pipeline useless until the frozen point can be identified and cleared. Furthermore, due to the variability of the moisture content and the complete lack of suitable and affordable measurement equipment, wet gas is being used as the pricing standard in the natural gas industry, leading to pricing errors of up to 1.74%. The proposed battery- or solar-powered sensors will permit unattended operation and data transmission capability and will be installed at the natural gas wellheads as well as different points along the distribution network where these types of measurements are in high demand.