SBIR-STTR Award

An Instrumental Platform for Identifying, Collecting, and Analyzing Particles with Micron and Submicron Dimensions
Award last edited on: 1/5/2023

Sponsored Program
SBIR
Awarding Agency
DOE
Total Award Amount
$1,349,931
Award Phase
2
Solicitation Topic Code
06c
Principal Investigator
Kristin Di Bona

Company Information

Wyonics LLC

1321 East Park Avenue
Laramie, WY 82070
   (205) 239-0219
   krdibona@wyonics.com
   www.wyonics.com
Location: Single
Congr. District: 00
County: Albany

Phase I

Contract Number: DE-SC0021868
Start Date: 6/28/2021    Completed: 3/27/2022
Phase I year
2021
Phase I Amount
$200,000
As microanalytical techniques advance and modern technologies continue to miniaturize, there exists a growing need for particle manipulation instrumentation with greater resolution and specific selectivity on a small micrometer (?m) to nanometer (nm) scale. The need for an instrumental platform which can spatially resolve ?m-sized particles is apparent in microanalytical fields, such as nuclear forensics and semiconductors, which require the identification of micron-sized particles and non-destructive relocation to enable sequential analyses via several complementary analytical platforms. Advanced manufacturing industries, such as microelectronics, would also benefit from ?m- to nm-scale particle manipulation and analysis technologies to generate advanced materials and remove contaminants. An instrumental platform has been designed with the ability to efficiently identify particles of interest on a sample with ?m- to nm-scale precision, collect the particles in a non-destructive, non- contaminating manner, and relocate them to another location for placement or further analyses. The platform employs a simple, elegant approach combining optical imaging for fast particle identification with a micromanipulation system for particle relocation. Software will be developed to both manually and electronically identify and manipulate particles of interest for the desired application. An instrumental platform will be designed and constructed with the capability to identify individual particles of refractory materials with dimensions between 0.1 and 1000 ?m, collect said particles, and relocate the particles to another location for further analysis. Software will be developed for instrumental control in a manual, interactive mode which allows control of the particle relocation and generation of analytical data via the optical system. Additional software will be developed to enable the automatic location and collection of specific particles and images without the need for constant user input. The instrumental platform, along with the accompanying software, will be tested using well- suited model systems for further development, modification, and optimization. The described instrumental platform is customizable and directly applicable to many commercial industries and advanced sectors, including microanalytical fields such as nuclear forensics (identified by the U.S. Department of Energy), advanced technology manufacturers, such as semiconductors, electronics, smart materials, and sensor technologies, and academic laboratories. Microanalytical industries will benefit by the improved resolution of the platform and the ability to manipulate specific particles in a non-destructive, non-contaminating manner. The developed instrumentation can also improve a variety of micro- and nano-technologies by providing a platform which can non-destructively rearrange particulate materials in desired patterns without contamination. Phase II efforts will focus on the optimization and prototyping as well as customer and beta-tester identification for the platform.

Phase II

Contract Number: DE-SC0021868
Start Date: 8/22/2022    Completed: 8/21/2024
Phase II year
2022
Phase II Amount
$1,149,931
1. Problem Statement Many technological fields would benefit greatly from an instrumental platform capable manipulating particles with µm- to nm-scale dimensions in a non-destructive, non-contaminating manner. A prime example is the field of nuclear forensics, where the elemental/isotopic analysis of individual µm-scale particles of actinide-containing materials is critical to ongoing nuclear non- proliferation efforts. The ability to accurately identify, collect, and relocate individual µm-scale particles thus plays a direct role in ensuring national security, but more broadly these capabilities are increasingly desired across a wide variety of technological sectors where the need to fabricate and manipulate materials on smaller and smaller length scales continues to increase. 2. Overall Approach An instrumental platform has been designed with the ability to efficiently locate individual µm- to nm-scale particles, collect said particles in a non-destructive, non-contaminating manner, and relocate the particles to another substrate for further analysis. The platform employs a simple, widely applicable approach combining optical imaging for fast particle identification and a micromanipulation system for particle relocation, both controlled through custom software capable of automating many aspects of the particle manipulation process. 3. Phase I Accomplishments An instrumental platform was constructed and shown to be capable of identifying individual particles of refractory materials with dimensions between 0.1 and 1000 µm, collecting specific particles, and relocating them to another location for further analysis. The developed micromanipulation platform was evaluated using relevant model particle systems and found to be fast and highly reproducible. Phase I thoroughly demonstrated the feasibility of the proposed technology, showing that it can serve as an ideal tool for the manipulation of µm-scale particles and is compatible with any desired ex situ analytical methods. 4. Phase II Work Plan Phase II will focus on the continued development of the manipulation platform demonstrated in Phase I with the ultimate goal of producing a functional prototype system for commercialization. The developed system will be optimized using particle systems relevant to customer needs. Prototyping, software development, customer outreach, and beta-testing in Phase II will produce a robust commercial-ready platform, capable of meeting the needs of current and emerging high- tech applications. 5. Commercial Application, Benefits The described instrumental platform is customizable and directly applicable to many commercial industries and advanced sectors, including microanalytical fields such as semiconductors, electronics, smart materials, sensors, and nanotechnology. Industries will benefit from the platform’s ability to manipulate specific particles in a nondestructive, noncontaminating manner, enabling the development of domestic high tech manufacturing economies. The developed instrumentation will enable a variety of micro- and nanotechnologies by providing a platform which can nondestructively rearrange particulate materials in desired patterns without contamination.