SBIR-STTR Award

Glass-metal Fritted Assemblies for Alpha-detection
Award last edited on: 1/5/2023

Sponsored Program
SBIR
Awarding Agency
DOE
Total Award Amount
$1,298,916
Award Phase
2
Solicitation Topic Code
C52-02b
Principal Investigator
David Botros

Company Information

Incom Inc

294 Southbridge Road
Charlton, MA 01507
   (508) 765-9151
   sales@incomusa.com
   www.incomusa.com
Location: Single
Congr. District: 01
County: Worcester

Phase I

Contract Number: DE-SC0021773
Start Date: 6/28/2021    Completed: 4/27/2022
Phase I year
2021
Phase I Amount
$199,078
Nuclear physics research has a need for fast neutron imaging of objects that are several mean-free-paths thick. For the associated particle imaging technique to work, sufficiently fast and high spatial resolution alpha-particle imaging is required. Alpha particles are generated in the fusion reaction that creates the neutron as well. By tracking the location and timestamp of these alpha particle detection events, one has information on the initial direction and creation time of that neutron. While conventional in-vacuum scintillators and air-side position-sensitive light sensors are up to the task, getting the light through the vacuum window without loss of spatial resolution remains a key challenge. This vacuum barrier must withstand high temperature vacuum bake, be made of materials compatible with welding to the neutron generator target assembly and maintain vacuum integrity for a workable neutron generator. Using fiberoptic faceplates that present a zero optical thickness approach and maintain spatial resolution is a demonstrated approach, but the component yield has been small and there is insufficient commercial interest due to the size of the current market. Initial Phase I development will demonstrate proof of concept success for the proposed application, Custom Fiber Optic plate (FOP) windows will be fabricatedutilizing a fiber packing structure in a “half-hex” methodology and bonded to a mating alloy flange that will closely match the FOP’s coefficient of thermal expansion (CTE). Furthermore, this approach, along with developing a Hot Isostatic Pressing process to frit seal the matching CTE alloy flanges to a fiberoptic plate will help mitigate fracturing of frit seals in the final assembly. Stronger bonding from HIP fusing and closer matching CTE will allow the assembly to be welded into a stainless-steel housing and baked out at 350 C for an extended (>1 day) period without the loss of the vacuum. A successful effort to develop a hermetic glass-metal seal for a 50-mm or greater diameter fiber-optic faceplate that can withstand the rigors of neutron generator fabrication helps to advance the associated particle imaging (API) D-T neutron generator state-of-the-art. The development of portable, high-output API D-T neutron generators can make neutron imaging a viable diagnostic tool for applications that require imaging of thick, dense objects with high-Z materials for which X-ray imaging is infeasible.

Phase II

Contract Number: DE-SC0021773
Start Date: 8/22/2022    Completed: 8/21/2024
Phase II year
2022
Phase II Amount
$1,099,838
Problem Being Addressed – Nuclear physics research has a need for fast neutron imaging of objects that are several mean-free-paths thick. For the associated particle imaging technique to work, sufficiently fast and high spatial resolution alpha-particle imaging is required. Alpha particles are generated in the fusion reaction that creates the neutron as well. By tracking the location and timestamp of these alpha particle detection events, one has information on the initial direction and creation time of that neutron. While conventional in-vacuum scintillators and air-side position-sensitive light sensors are up to the task, getting the light through the vacuum window without loss of spatial resolution remains a key challenge. This vacuum barrier must withstand high temperature vacuum bake, be made of materials compatible with welding to the neutron generator target assembly and maintain vacuum integrity for a workable neutron generator. Using fiberoptic faceplates that present a zero optical thickness approach and maintain spatial resolution is a demonstrated approach, but the component yield has been small and there is insufficient commercial interest due to the size of the current market. How Problem is Being Addressed –Phase II development will demonstrate repeated feasibility for a 50mm success for the proposed application, Custom Fiber Optic plate (FOP) windows will be fabricated utilizing a fiber packing structure in a “half-hex” methodology and bonded to a mating alloy flange that will closely match the FOP’s coefficient of thermal expansion (CTE). Custom solid frit rings and upgraded facilities will establish Pilot production for 65mm FOP fritted to alloy flanges. Furthermore,this approach, along with developing a Hot Isostatic Pressing process to frit seal the matching CTE alloy flanges to a fiberoptic plate will help mitigate fracturing of frit seals in the final assembly. Stronger bonding from HIP fusing and closer matching CTE will allow the assembly to be welded into a stainless- steel housing and baked out at 350 C for an extended (>1 day) period without the loss of the vacuum. Commercial Applications – A successful effort to develop a hermetic glass-metal seal for a 50mm & 65mm diameter fiber-optic faceplates that can withstand the rigors of neutron generator fabrication helps to advance the associated particle imaging (API) D-T neutron generator state-of-the-art.Thedevelopment of portable, high-output API D-T neutron generators can make neutron imaging a viable diagnostic tool for applications that require imaging of thick, dense objects with high-Z materials for which X-ray imaging is infeasible.