SBIR-STTR Award

Resistive Coatings for High-Performance, Low-Background MCPs Operating Across Broad Temperature Ranges and at Cryogenic Temperatures
Award last edited on: 10/23/2024

Sponsored Program
SBIR
Awarding Agency
DOE
Total Award Amount
$2,299,332
Award Phase
2
Solicitation Topic Code
29
Principal Investigator
Till Cremer

Company Information

Incom Inc

294 Southbridge Road
Charlton, MA 01507
   (508) 765-9151
   sales@incomusa.com
   www.incomusa.com
Location: Single
Congr. District: 01
County: Worcester

Phase I

Contract Number: DE-SC0015729
Start Date: 6/13/2016    Completed: 3/12/2017
Phase I year
2016
Phase I Amount
$149,846
The planned “Deep Underground Neutrino Experiment” (DUNE), will become the premier High Energy Physics (HEP) Neutrino Physics research facility in the world, and will be constructed over the coming decade. DUNE and its associated short-baseline surface neutrino detectors will be enormous Liquid Argon T ime Projection Chambers, recording tracks from neutrino interaction secondary particles in exquisite detail by drifting patterns of ionization charge through giant vats of ultrapure cryogenic noble liquid. Photon detection systems will play a crucial role in DUNE and its associated neutrino experiments, but requirements for the cost-effective large-area photosensors needed to collect very hard VUV light in Liquid Argon environment are very demanding. Over the last decade we have developed a room-temperature baseline Large Area Picosecond Photon Detectors (LAPPDTM), a 203 mm x 203 mm flat photosensor with unsurpassed photon timing accuracy. The core element of this detector is Incom’s next generation microchannel plate (MCP) technology, which was also developed within the DOE-supported LAPPD consortium. Herein, we propose to develop a new generation of MCPs with improved thermo-electrical properties, specifically addressing undesired resistance changes with temperature. The resulting MCPs will have superior voltage and gain stability, be less prone to thermal runaway, and can be further optimized to operate reliably at cryogenic temperatures. Other applications such as space science instrumentation, field-deployed radiation detectors for homeland security applications as well as industrial high and low-temperature applications such as the mining or oil prospecting industry are expected to benefit from this development. In Phase I, working closely with Argonne National Laboratory and University of California, Berkeley – Space Science Laboratories, we propose proof-of-concept demonstration of resistive coatings that exhibit an extremely low, or negligible temperature coefficient of resistance. In Phase II we will apply these coatings to fabricate MCPs that exhibit stable gain and resistance over wide temperature ranges, and that can be optimized to reliably operate at cryogenic or elevated temperatures. This innovation will enable new detector plications in HEP, nuclear physics, spectroscopy, and calorimetry applications, as well as in medical imaging, homeland security, and energy sectors. Key words: LAPPDTM, High Energy Physics, cryogenic particle detector, thermal runaway, atomic layer deposition, temperature coefficient of resistance, TCR, microchannel plates, MCP.

Phase II

Contract Number: DE-SC0018778
Start Date: 8/19/2019    Completed: 8/18/2021
Phase II year
2019
(last award dollars: 2022)
Phase II Amount
$2,149,486

Proliferation detection equipment requires deployment at remote, inaccessible sites and has to be able to operate over a rather wide temperature range.Scintillation light due to neutrons, gamma rays, or other indicators of nuclear material is typically detected with photon sensors based on photocathodes and microchannel?plate (MCP) amplifiers.Incom’s MCP technology uses an Atomic Layer Deposition (ALD) process to impart resistive and emissive properties to Glass Capillary Array (GCA) substrates.This offers the unique opportunity of tuning the thermo?electrical properties of the resistive layer, which is not possible with conventional MCPs.We propose to develop MCPs with optimized resistive coatings that can operate at ultra?high count rates in high background environments, and across broad temperature ranges.This development will afford photodetectors that operate stably over a broad temperature range, and to enable “lowpower” LAPPDs by using the low?TCR MCPs in low gain mode.In Phase I of this program we were able to show that for Incom’s baseline resistive material, Chem1, the TCR of ALD?GCA?MCPs can be adjusted by changing the material composition.We evaluated that the TCR of Chem1 can be significantly improved through ALD process optimization.We also developed a new tunable resistance material with an even lower TCR value of ?0.01 K?1.Qualification trials using GCA substrates are needed to further qualify this materials potential.In Phase II our work will be threefold; we will a) optimize our current tunable resistance material, Chem1, to achieve the lowest possible TCR for this material, b) qualify a new material developed in Phase I at Argonne for its applicability to MCPs, and c) continue the development of new materials.Potential applications that would benefit from stable, high?dynamic range ALD?GCA?MCPs include a wide variety of sensors for space flight instrumentation, time?of?flight mass spectrometers, PET scanners, Proton radiography, as well as high?temperature (T ? 200° C) PMTs for mining and oil prospecting applications.